University Of Pune Question Paper
Fourth Year B.Pharm. Examination, 2010
PHARMACEUTICAL ANALYSIS – III
(2004 Course)
Time : 3 Hours Max. Marks : 80
Instructions : 1) Question No. 1 and 5 are compulsory.
2) Out of the remaining, attempt two questions from Section I
and two questions from Section II.
3) Answers to the two Sections should be written in separate
answer books.
4) Figures to the right indicate full marks.
5) Draw well labeled diagrams wherever necessary.
SECTION – I
1. a) Describe various sample handling techniques for solid sample in IR. 5
b) Discuss types of molecular vibrations in IR. 5
2. a) Explain fragmentation modes in mass spectroscopy. 7
b) Explain in brief C13 NMR and NOE. 8
3. a) Discuss system suitability parameter as per USP. 5
b) Write a note on instrumentation of Atomic absorption spectroscopy. 5
c) Give the principle of ESR. 5
4. Write short notes on any three : 15
a) Chemical shift.
b) X-ray diffraction techniques.
c) Interference in flame photometry.
d) Raman spectroscopy.
SECTION – II
5. a) State various detectors used in gas chromatography. 6
b) Explain in brief theory of gas chromatography. 4
6. a) Explain various pumps used in HPLC. 7
b) Discuss in brief on quantization technique and degassing techniques in HPLC. 8
7. a) Give the principle and application of super critical fluid extraction. 8
b) Explain in brief on centrifugal TLC and Horizontal TLC. 7
8. Write short notes on any three : 15
a) Measurement of Radioactivity.
b) Application of HPTLC.
c) Types of development in Electrophorosis.
d) ENDOR and ELDOR.
————————
Fourth Year B.Pharm. Examination, 2010
PHARMACEUTICAL ANALYSIS – III
(2004 Course)
Time : 3 Hours Max. Marks : 80
Instructions : 1) Question No. 1 and 5 are compulsory.
2) Out of the remaining, attempt two questions from Section I
and two questions from Section II.
3) Answers to the two Sections should be written in separate
answer books.
4) Figures to the right indicate full marks.
5) Draw well labeled diagrams wherever necessary.
SECTION – I
1. a) Describe various sample handling techniques for solid sample in IR. 5
b) Discuss types of molecular vibrations in IR. 5
2. a) Explain fragmentation modes in mass spectroscopy. 7
b) Explain in brief C13 NMR and NOE. 8
3. a) Discuss system suitability parameter as per USP. 5
b) Write a note on instrumentation of Atomic absorption spectroscopy. 5
c) Give the principle of ESR. 5
4. Write short notes on any three : 15
a) Chemical shift.
b) X-ray diffraction techniques.
c) Interference in flame photometry.
d) Raman spectroscopy.
SECTION – II
5. a) State various detectors used in gas chromatography. 6
b) Explain in brief theory of gas chromatography. 4
6. a) Explain various pumps used in HPLC. 7
b) Discuss in brief on quantization technique and degassing techniques in HPLC. 8
7. a) Give the principle and application of super critical fluid extraction. 8
b) Explain in brief on centrifugal TLC and Horizontal TLC. 7
8. Write short notes on any three : 15
a) Measurement of Radioactivity.
b) Application of HPTLC.
c) Types of development in Electrophorosis.
d) ENDOR and ELDOR.
————————
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