PHARMACEUTICAL ANALYSIS – III,University Of Pune Question Paper,2010 Question Paper,Fourth Year B.Pharm.

University Of Pune Question Paper
Fourth Year B.Pharm. Examination, 2010
PHARMACEUTICAL ANALYSIS – III
(2004 Course)
Time : 3 Hours Max. Marks : 80
 Instructions : 1) Question No. 1 and 5 are compulsory.
2) Out of the remaining, attempt two questions from Section I
and two questions from Section II.
3) Answers to the two Sections should be written in separate
answer books.
4) Figures to the right indicate full marks.
5) Draw well labeled diagrams wherever necessary.
SECTION – I
1. a) Describe various sample handling techniques for solid sample in IR. 5
b) Discuss types of molecular vibrations in IR. 5
2. a) Explain fragmentation modes in mass spectroscopy. 7
b) Explain in brief C13 NMR and NOE. 8
3. a) Discuss system suitability parameter as per USP. 5
b) Write a note on instrumentation of Atomic absorption spectroscopy. 5
c) Give the principle of ESR. 5
4. Write short notes on any three : 15
a) Chemical shift.
b) X-ray diffraction techniques.
c) Interference in flame photometry.
d) Raman spectroscopy.
SECTION – II
5. a) State various detectors used in gas chromatography. 6
b) Explain in brief theory of gas chromatography. 4
6. a) Explain various pumps used in HPLC. 7
b) Discuss in brief on quantization technique and degassing techniques in HPLC. 8
7. a) Give the principle and application of super critical fluid extraction. 8
b) Explain in brief on centrifugal TLC and Horizontal TLC. 7
8. Write short notes on any three : 15
a) Measurement of Radioactivity.
b) Application of HPTLC.
c) Types of development in Electrophorosis.
d) ENDOR and ELDOR.
————————

Fourth Year B.Pharm.,University Of Pune Question Paper,2010 Question Paper,PHARMACEUTICAL JURISPRUDENCE AND REGULATORY AFFAIRS

University Of Pune Question Paper
Fourth Year B.Pharm. Examination, 2010
PHARMACEUTICAL JURISPRUDENCE AND REGULATORY AFFAIRS
(2004 Course)
Time : 3 Hours
Max. Marks : 80
 Instructions: 1) Question Nos. 1 and 5 are compulsory. Out of remaining,
attempt 2 questions from Section I and 2 questions from
Section II.
2) Answers to the two Sections should be written in separate
books.
3) Figures to the right indicate full marks.
SECTION – I
1. Define “Illicit Traffic”. Discuss power of Central Government to permit, control
and regulate certain operations under NDPS 1985. 10
2. A) What are the qualifications and duties of Drug Inspector ? Give procedure of
Inspections. 9
B) Discuss the requirements of Non-bonded Laboratory. Write procedure for
obtaining rectified spirite under Non-bonded Laboratory. 6
3. A) Define ‘Advertisement’. Describe the provisions pertaining classes of
prohibited advertisement and Exempted advertisement. 10
B) Differentiate in between State and Joint State Pharmacy Council under Pharmacy
Act 1948. 5
4. Write short notes on (any three) : 15
1) Industrial Safety and Health
2) Consumer Protection Act
3) Public Analyst
4) D.T.A.B.
SECTION – II
5. A) Define Patents. Discuss in brief the filling and processing of Patents. 7
B) Define IPR, add note on Trade marks. 3
6. A) Discuss in brief about 8
a) Europe-European Agency for the Evaluation of medicinal product.
b) Medicine Control Agency
B) Discuss ICH Guidelines. 7
7. A) Discuss in brief salient features of Indian Patents Act 1970. 7
B) Differentiate between NDA and ANDA. Write note on ‘contents of ANDA. 8
8. Write short note on (any three) : 15
1) US-FDA
2) Exclusive Marketing Right
3) Patent infringement
4) TGA.
————————